N-苯甲酰基-4-甲基-苯磺酰胺合成路线 （共 56 条）
反应条件
pyridine; iodosylbenzene; iron(II) chloride in dichloromethane
T=20°C; 18 h; Molecular sieveInert atmosphere;
参考文献
Ton, Thi My Uyen; Tejo, Ciputra; Tania, Stefani; Chang, Joyce Wei Wei; Chan, Philip Wai Hong
Journal of Organic Chemistry, 2011 , vol. 76, # 12 p. 4894 - 4904
反应条件
pyridine; [bis(acetoxy)iodo]benzene; iron(II) chloride in dichloromethane
T=20°C; 18 h; Inert atmosphereMolecular sieve;
参考文献
Ton, Thi My Uyen; Tejo, Ciputra; Tania, Stefani; Chang, Joyce Wei Wei; Chan, Philip Wai Hong
Journal of Organic Chemistry, 2011 , vol. 76, # 12 p. 4894 - 4904
反应条件
1: CH2Cl2 / 10 h / 20 °C
2: 92 percent / AlCl3 / CH2Cl2 / 15 h / 20 °C
View Scheme
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
1: 10 h / 40 °C
2: 92 percent / AlCl3 / CH2Cl2 / 15 h / 20 °C
View Scheme
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
1: 87 percent / triethylamine / benzene / 14 h / Ambient temperature
2: 90 percent / O2, t-BuOK / dimethylsulfoxide / 0.17 h / Ambient temperature
View Scheme
参考文献
Yijima, Chino; Hino, Fumio; Suda, Kohji
Synthesis, 1981 , # 8 p. 610 - 611
反应条件
potassium carbonate
0.333333 h; Heating;
参考文献
Ludwig, Miroslav; Parik, Patrik; Kulhanek, Jiri
Collection of Czechoslovak Chemical Communications, 1995 , vol. 60, # 5 p. 841 - 850
反应条件
1.1: LiAlHSeH / tetrahydrofuran
1.2: I2; KI / tetrahydrofuran
2.1: 96 percent / iPr2NEt; piperidine / acetonitrile / 0.08 h / 25 °C
View Scheme
参考文献
Surabhi, Prathima; Wu, Xinghua; Hu, Longqin
Tetrahedron Letters, 2006 , vol. 47, # 27 p. 4609 - 4613
反应条件
1: 87 percent / triethylamine / benzene / 14 h / Ambient temperature
2: 90 percent / O2, t-BuOK / dimethylsulfoxide / 0.17 h / Ambient temperature
View Scheme
参考文献
Yijima, Chino; Hino, Fumio; Suda, Kohji
Synthesis, 1981 , # 8 p. 610 - 611
反应条件
1: 75 percent / triethylamine
2: acetonitrile / 3 h / Ambient temperature
View Scheme
参考文献
Morkved, Eva H.; Cronyn, Marshall W.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 6 p. 381 - 388
反应条件
1: 60 percent / triethylamine / tetrahydrofuran / Ambient temperature
2: 75 percent / triethylamine
3: acetonitrile / 3 h / Ambient temperature
View Scheme
参考文献
Morkved, Eva H.; Cronyn, Marshall W.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 6 p. 381 - 388
