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乙二醇
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63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-壬烷基丁酸酯
合成路线
（共 10 条）
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
117636-43-8
+
117636-46-1
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst T=20 - 25°C; pH=7.4; 8 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
117636-68-7
+
628-99-9
2-壬醇
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
117636-46-1
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
117636-58-5
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
117636-68-7
+
628-99-9
2-壬醇
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
117636-46-1
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
117636-58-5
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
69727-42-0
2-壬烷基丁酸酯
→
反应条件
628-99-9
2-壬醇
+
70419-06-6
(S)-(+)-2-壬醇
反应条件
1: Candida antarctica lipase B immobilized on acrylic resin catalyst / 8 h / 20 - 25 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction 2: Candida antarctica lipase B immobilized on acrylic resin catalyst / pentane / 48 h / 20 - 25 °C / Enzymatic reaction View Scheme
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
628-99-9
2-壬醇
+
141-75-3
丁酰氯
→
反应条件
69727-42-0
2-壬烷基丁酸酯
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine T=20°C; Cooling with ice;
参考文献
Strohalm, Hedwig; Dregus, Marta; Wahl, Astrid; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10339 - 10344
