3-氨基-4-甲氧基苯磺酰胺合成路线 （共 5 条）
反应条件
ammonium hydroxide in water
T=0 - 50°C;
参考文献
Leonard, Kristi Anne; Zhang, Yan; Tounge, Brett Andrew; Wang, Aihua; Hawkins, Michael; Jackson, Paul Francis; Barbay, Joseph Kent; Maharoof, Umar S.M.
Patent: US2012/129872 A1, 2012 ;
Location in patent: Page/Page column 31 ;
参考文献
Goissedet; Despois
Patent: US2309841 , 1936 ;
反应条件
1: chlorosulfuric acid
2: aqueous ammonia
3: aqueous hydrochloric acid
View Scheme
参考文献
Adams; Long; Johanson
Journal of the American Chemical Society, 1939 , vol. 61, p. 2342,2344
反应条件
1: aqueous ammonia
2: aqueous hydrochloric acid
View Scheme
参考文献
Adams; Long; Johanson
Journal of the American Chemical Society, 1939 , vol. 61, p. 2342,2344
反应条件
thionyl chloride; triethylamine
1.) 45 deg C, 6 h 2.) 18 deg C, 15 h;
参考文献
Porte, Catherine; Borrin, Roland; Bouma, Sophie; Delacroix, Alain
Bulletin de la Societe Chimique de France, 1982 , vol. 1, # 3-4 p. 90 - 96
