pyridinium chlorochromate in dichloromethane T=20°C;
参考文献
Chu, Ling; Wang, Xiao-Chen; Moore, Curtis E.; Rheingold, Arnold L.; Yu, Jin-Quan
Journal of the American Chemical Society, 2013 , vol. 135, # 44 p. 16344 - 16347
1: thiophene With 2-Chloro-2-methylpropane; lithium in tetrahydrofuran
0.75 h; sonication;
2: thiophene-2-carbaldehyde in tetrahydrofuran
1 h;
参考文献
Sanchez, Muriel; Diallo, Ousmane; Oussaid, Adyl; Oussaid, Boualem; Garrigues, Bernard
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 173, p. 235 - 242
1: thien-2-yl bromide With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h; Inert atmosphere;
2: thiophene-2-carbaldehyde in tetrahydrofuran; hexane
T=-78°C; 1 h; Inert atmosphere;
参考文献
Chu, Ling; Wang, Xiao-Chen; Moore, Curtis E.; Rheingold, Arnold L.; Yu, Jin-Quan
Journal of the American Chemical Society, 2013 , vol. 135, # 44 p. 16344 - 16347
