6-氨基-1,4-二氢-2,3-喹喔啉二酮合成路线 （共 10 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol; ethyl acetate
P=1551.44 Torr;
参考文献
Chambers, James J.; Gouda, Hiroaki; Young, David M.; Kuntz, Irwin D.; England, Pamela M.
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 13886 - 13887
反应条件
1: 86 percent / 24 h / Heating
2: 90 percent / H2 / Pd/C / ethyl acetate; ethanol / 1551.44 Torr
View Scheme
参考文献
Chambers, James J.; Gouda, Hiroaki; Young, David M.; Kuntz, Irwin D.; England, Pamela M.
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 13886 - 13887
反应条件
ytterbium triflare
T=80°C; Phillips reaction; 1 h;
参考文献
Wang, Limin; Liu, Jijun; Tian, He; Qian, Changtao
Synthetic Communications, 2004 , vol. 34, # 8 p. 1349 - 1357
反应条件
ammonium formate; palladium on activated charcoal
参考文献
Lubisch; Behl; Hofmann
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2887 - 2892
反应条件
1: KNO3, H2SO4
2: HCOONH4 / Pd/C
View Scheme
参考文献
Lubisch; Behl; Hofmann
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2887 - 2892
反应条件
1: Fe, AcOH / Heating
2: KNO3, H2SO4
3: HCOONH4 / Pd/C
View Scheme
参考文献
Lubisch; Behl; Hofmann
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2887 - 2892
反应条件
2: Fe, AcOH / Heating
3: KNO3, H2SO4
4: HCOONH4 / Pd/C
View Scheme
参考文献
Lubisch; Behl; Hofmann
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2887 - 2892
反应条件
1: NH2
3: Fe, AcOH / Heating
4: KNO3, H2SO4
5: HCOONH4 / Pd/C
View Scheme
参考文献
Lubisch; Behl; Hofmann
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2887 - 2892
参考文献
Mager; Berends
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 5,17
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Gallinek
Patent: DE77348 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 1151
