叔丁基二甲硅基三氟甲磺酸酯合成路线 （共 109 条）
反应条件
triethylamine in dichloromethane
0.0833333 h; Yield given. Yields of byproduct given;
参考文献
Mander, Lewis N.; Sethi, S. Paul
Tetrahedron Letters, 1984 , vol. 25, # 51 p. 5953 - 5956
反应条件
2,6-dimethylpyridine in dichloromethane
T=-78°C; 1.5 h;
参考文献
Roush, William R; Barda, David A; Limberakis, Chris; Kunz, Roxanne K
Tetrahedron, 2002 , vol. 58, # 32 p. 6433 - 6454
反应条件
triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Collins, Karl D.; Ruehling, Andreas; Lied, Fabian; Glorius, Frank
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3800 - 3805
反应条件
lithium hexamethyldisilazane
1.) THF, hexane, -78 deg C, 45 min, 2.) THF, -78 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Wiberg, Kenneth B.; Snoonian, John R.
Journal of Organic Chemistry, 1998 , vol. 63, # 5 p. 1390 - 1401
反应条件
sodium methylate
1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Oriyama, Takeshi; Noda, Kojiro; Sugawara, Satomi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2217 - 2223
反应条件
sodium methylate
1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Oriyama, Takeshi; Noda, Kojiro; Sugawara, Satomi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2217 - 2223
反应条件
sodium methylate
1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Oriyama, Takeshi; Noda, Kojiro; Sugawara, Satomi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2217 - 2223
反应条件
1: 95 percent / pyridine
2: 82 percent / 80percent acetic acid
View Scheme
参考文献
Bohringer; Graff; Caruthers
Tetrahedron Letters, 1993 , vol. 34, # 17 p. 2723 - 2726
反应条件
1: 81 percent / 2,6-lutidine / CH2Cl2 / 0.08 h / 0 °C
2: 77 percent / aq. CAN / acetonitrile / 0.25 h / 0 °C
View Scheme
参考文献
Fujishima, Toshie; Kittaka, Atsushi; Yamaoka, Kazuyoshi; Takeyama, Ken-Ichi; Kato, Shigeaki; Takayama, Hiroaki
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 11 p. 1863 - 1869
