叔丁基二甲硅基三氟甲磺酸酯合成路线 （共 109 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide T=0°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 5 p. 619 - 622
参考文献
Burns, Christopher J.; Dankulich, William P.; McGarry, Daniel G.; Volz, Francis A.
Patent: US2002/193410 A1, 2002 ;
US 20020193410 A1
反应条件
1: 3-bromopropan-1-ol With 2,6-dimethylpyridine; CaH2 in dichloromethane T=0°C; Inert atmosphere; 2: t-butyldimethylsiyl triflate in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Kong, Biao; Tang, Jing; Wu, Zhangxiong; Wei, Jing; Wu, Hao; Wang, Yongcheng; Zheng, Gengfeng; Zhao, Dongyuan
Angewandte Chemie - International Edition, 2014 , vol. 53, # 11 p. 2988 - 2992
Angew. Chem., 2014 , vol. 53, # 11 p. 3
反应条件
triethylamine in dichloromethane 0.75 h; Ambient temperature;
参考文献
Moreno, Maria Jose S. M.; Martins, Rosa Maria L. M.; Sa E Melo, Maria Luisa; Campos Neves, Andre S.
Chemistry Letters, 1997 , # 6 p. 529 - 530
反应条件
in chloroform-d1 T=20°C;
参考文献
Bartoszewicz, Agnieszka; Kalek, Marcin; Stawinski, Jacek
Tetrahedron, 2008 , vol. 64, # 37 p. 8843 - 8850
反应条件
sodium methylate 1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Synthetic Communications, , vol. 29, # 13 p. 2217 - 2223
反应条件
1: 73 percent / Et3N / CH2Cl2 / 2 h / Heating 2: 93 percent / LiAlH4 / diethyl ether / -100 - -10 °C View Scheme
参考文献
Dalla; Catteau
Tetrahedron, 1999 , vol. 55, # 21 p. 6497 - 6510
参考文献
Journal of Organic Chemistry, , vol. 49, # 10 p. 1772 - 1783
反应条件
triethylamine in dichloromethane T=23°C; Product distribution;
参考文献
Tetrahedron Letters, , vol. 34, # 39 p. 6215 - 6218
反应条件
dimethylsulfide; triethylamine 1.) CH2Cl2, -50 deg C, 30 min 2.) -50 deg C, 1h; Yield given. Multistep reaction;
参考文献
Kim; Kee
Tetrahedron Letters, 1990 , vol. 31, # 20 p. 2899 - 2900
