叔丁基二甲硅基三氟甲磺酸酯合成路线 （共 109 条）
反应条件
triethylamine in dichloromethane T=0°C; 1.5 h; Inert atmosphere;
参考文献
Chepiga, Kathryn M.; Feng, Yan; Brunelli, Nicholas A.; Jones, Christopher W.; Davies, Huw M. L.
Organic Letters, 2013 , vol. 15, # 24 p. 6136 - 6139
反应条件
2,6-dimethylpyridine
参考文献
Keenan, Richard M.; Eppley, Daniel F.; Tomaszek, Thaddeus A.
Tetrahedron Letters, 1995 , vol. 36, # 6 p. 819 - 822
反应条件
2,6-dimethylpyridine in dichloromethane T=-40°C; Inert atmosphere;
参考文献
Hatakeyama, Susumi; Yoshino, Madoka; Eto, Kohei; Takahashi, Keisuke; Ishihara, Jun; Ono, Yoshiyuki; Saito, Hitoshi; Kubodera, Noboru
Journal of Steroid Biochemistry and Molecular Biology, 2010 , vol. 121, # 1-2 p. 25 - 28
反应条件
1: 92 percent / pyridine / 4 h / -35 °C 2: In; aq. NH4Cl / methanol / 18 h / 20 °C View Scheme
参考文献
Pitts; Harrison; Moody
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 955 - 977
反应条件
n-butyllithium 1.) THF, hexane, -75 deg C, 15 min, 2.) -75 deg C -> room temperature, overnight; Yield given. Multistep reaction;
参考文献
Dondoni, Alessandro; Douglas, Alan W.; Shinkai, Ichiro
Journal of Organic Chemistry, 1993 , vol. 58, # 11 p. 3196 - 3200
反应条件
pyridine 1.) (ClCH2)2, 0-25 degC, 12 h 2.) (ClCH2)2, 0 degC, 1 h.; Yield given. Multistep reaction;
参考文献
Nambiar, Sudhir; Daeuble, John F.; Doyle, Ronald J.; Taylor, K. Grant
Tetrahedron Letters, 1989 , vol. 30, # 17 p. 2179 - 2182
反应条件
2,6-dimethylpyridine in dichloromethane 0.366667 h;
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 13 p. 2011 - 2032
反应条件
dimethylsulfide; triethylamine 1.) CH2Cl2, -50 deg C, 30 min 2.) -50 deg C, 1h; Yield given. Multistep reaction;
参考文献
Kim; Kee
Tetrahedron Letters, 1990 , vol. 31, # 20 p. 2899 - 2900
反应条件
2,6-dimethylpyridine 1.) dichloromethane, room t., 2 h; 2.) 0 degC, 2 h; Yield given. Multistep reaction;
参考文献
Franck, Xavier; Figadere, Bruno; Cave, Andre
Tetrahedron Letters, 1995 , vol. 36, # 5 p. 711 - 714
反应条件
1H-imidazole in N,N-dimethyl-formamide T=0 - 20°C; 2 h;
参考文献
Bouamaied, Imenne; Stulz, Eugen
Synlett, 2004 , # 9 p. 1579 - 1583
