叔丁基二甲硅基三氟甲磺酸酯合成路线 （共 109 条）
反应条件
sodium methylate 1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Oriyama, Takeshi; Noda, Kojiro; Sugawara, Satomi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2217 - 2223
反应条件
2,6-dimethylpyridine in tetrahydrofuran; dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Enders, Dieter; Terteryan, Violeta; Paleek, Jii
Synthesis, 2010 , # 17 art. no. Z13010SS, p. 2979 - 2984
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Collins, Karl D.; Ruehling, Andreas; Lied, Fabian; Glorius, Frank
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3800 - 3805
反应条件
2,6-dimethylpyridine in dichloromethane T=0°C; 1 h;
参考文献
Takeuchi, Ken'ichi; Kitagawa, Toshikazu; Ohga, Yasushi; Yoshida, Masayasu; Akiyama, Fumio; Tsugeno, Akio
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 280 - 291
反应条件
2,6-dimethylpyridine in dichloromethane T=0 - 20°C; 3 h;
参考文献
LAUTENS, Mark; FAYOL, Aude; NAGAMOCHI, Masatoshi; FANG, Yuanqing
Patent: WO2007/134421 A1, 2007 ;
Location in patent: Page/Page column 150 ;
反应条件
1: 92 percent / pyridine / 4 h / -35 °C 2: In; aq. NH4Cl / methanol / 18 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 9 p. 955 - 977
反应条件
2,6-dimethylpyridine in dichloromethane T=0 - 20°C; 2 h;
参考文献
Dubbaka, Srinivas Reddy; Steunenberg, Peter; Vogel, Pierre
Synlett, 2004 , # 7 p. 1235 - 1238
反应条件
2,6-dimethylpyridine 1.) dichloromethane, room t., 2 h; 2.) 0 degC, 2 h; Yield given. Multistep reaction;
参考文献
Franck, Xavier; Figadere, Bruno; Cave, Andre
Tetrahedron Letters, 1995 , vol. 36, # 5 p. 711 - 714
反应条件
4-(N,N-dimethlyamino)pyridine; 2,6-di-tert-butyl-pyridine in dichloromethane T=-10°C; 3 h;
参考文献
Spivey, Alan C.; Martin, Laetitia J.; Grainger, Damian M.; Ortner, Joerg; White, Andrew J. P.
Organic Letters, 2006 , vol. 8, # 18 p. 3891 - 3894
反应条件
triethylamine in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Zhou, Jiacheng; Liu, Pingli; Lin, Qiyan; Metcalf, Brian W.; Meloni, David; Pan, Yongchun; Xia, Michael; Li, Mei; Yue, Tai-Yuen; Rodgers, James D.; Wang, Haisheng
Patent: US2010/190981 A1, 2010 ;
Location in patent: Page/Page column 67-68 ;
US 20100190981 A1
