N-(2-羟基乙基)三氟乙酰胺合成路线 (共 21 条)
反应条件
triethylamine in methanol T=0 - 20°C; Inert atmosphere;
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: WO2009/132310 A1, 2009 ;
Location in patent: Page/Page column 64 ;
参考文献
Bobkov, Georgii V.; Mikhailov, Sergey N.; Van Aerschot, Arthur; Herdewijn, Piet
Tetrahedron, 2008 , vol. 64, # 27 p. 6238 - 6251
反应条件
triethylamine in methanol
反应条件
in dichloromethane 0.5 h;
参考文献
Slama, James; Rando, Robert R.
Carbohydrate Research, 1981 , vol. 88, p. 213 - 222
反应条件
in methanol Ambient temperature;
参考文献
Norrild, Jens Chr.; Pedersen, Christian; Sotofte, Inger
Carbohydrate Research, 1997 , vol. 297, # 3 p. 261 - 272
反应条件
in diethyl ether 1 h;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 49 - 55
反应条件
in diethylene glycol dimethyl ether Ambient temperature;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 49 - 55
反应条件
in diethylene glycol dimethyl ether 1 h; Ambient temperature; Further byproducts given;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 49 - 55
反应条件
in dichloromethane T=20°C; 0.5 h;
参考文献
Synlett, , # 5 p. 755 - 758