N-(2-羟基乙基)三氟乙酰胺合成路线 (共 21 条)
反应条件
in diethylene glycol dimethyl ether 1 h; Ambient temperature; Further byproducts given;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 49 - 55
反应条件
in diethylene glycol dimethyl ether T=50°C; 0.5 h; Yield given. Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 87, # 1 p. 49 - 55
反应条件
in diethylene glycol dimethyl ether 1 h; Ambient temperature; Yield given. Further byproducts given;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 49 - 55
反应条件
in diethylene glycol dimethyl ether 1 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 87, # 1 p. 49 - 55
反应条件
in diethyl ether Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of Nondestructive Testing, , vol. 33, # 2 p. 265 - 272
参考文献
Russian Journal of Organic Chemistry, , vol. 48, # 10 p. 1289 - 1296
Zh. Org. Khim., , vol. 48, # 10 p. 1295 - 1301,7
反应条件
hydrogenchloride in diethyl ether 3 - 11 h; Reflux;
参考文献
Lobanova; Stankevich; Kukharev
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 10 p. 1289 - 1296
Zh. Org. Khim., 2012 , vol. 48, # 10 p. 1295 - 1301,7
反应条件
hydrogenchloride in diethyl ether 3 - 11 h; Reflux;
参考文献
Russian Journal of Organic Chemistry, , vol. 48, # 10 p. 1289 - 1296
Zh. Org. Khim., , vol. 48, # 10 p. 1295 - 1301,7
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Lazarus,R.A.; Benkovic,S.J.
Journal of the American Chemical Society, 1979 , vol. 101, p. 4300 - 4312
反应条件
p-toluenesulfonyl chloride; sodium iodide
1.) pyridine, 1 h, 4 deg C, overnight; 2.) butanone, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Slama, James; Rando, Robert R.
Carbohydrate Research, 1981 , vol. 88, p. 213 - 222