1-乙酰基-2,3,5-三苯甲酰氧基-1-beta-D-呋喃核糖合成路线 （共 164 条）
反应条件
in methanol; hexane; chloroform; ethyl acetate; acetonitrile
参考文献
The Regents of the University of Michigan
Patent: US5248672 A1, 1993 ;
反应条件
in methanol; hexane; chloroform; ethyl acetate; acetonitrile
参考文献
The Regents of the University of Michigan
Patent: US5574058 A1, 1996 ;
反应条件
1: With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=130°C; Vorbrueggen glycosylation; 0.0833333 h; microwave irradiation;
2: With ammonia in methanol
T=50°C; 16 h;
参考文献
Bookser, Brett C.; Raffaele, Nicholas B.
Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 173 - 179
反应条件
1: 99 percent / (CH3)3SiOSO2CF3 / 1,2-dichloro-ethane / 24 h / 24 °C
2: 82 percent / NH3 / methanol / 168 h / 24 °C
View Scheme
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1234 - 1255
