1-乙酰基-2,3,5-三苯甲酰氧基-1-beta-D-呋喃核糖合成路线 （共 164 条）
反应条件
trimethylsilylazide in dichloromethane T=20°C; Rearrangement; azidation; deacetylation; 3 h; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 324, # 3 p. 149 - 160
反应条件
tri-n-butyltin methoxide in dichloromethane
参考文献
Lengeler, David; Weisz, Klaus
Tetrahedron Letters, 2001 , vol. 42, # 8 p. 1479 - 1481
反应条件
boron trifluoride diethyl etherate in acetonitrile 48 h; Ambient temperature; Further byproducts given. Yields of byproduct given;
参考文献
Chavis; Grodenic; Imbach
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 3 p. 219 - 227
反应条件
boron trifluoride diethyl etherate in acetonitrile 3 h; Ambient temperature; Further byproducts given;
参考文献
European Journal of Medicinal Chemistry, , vol. 16, # 3 p. 219 - 227
反应条件
boron trifluoride diethyl etherate in acetonitrile 48 h; Ambient temperature; Further byproducts given. Yields of byproduct given;
参考文献
Chavis; Grodenic; Imbach
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 3 p. 219 - 227
反应条件
boron trifluoride diethyl etherate in acetonitrile 96 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Chavis; Grodenic; Imbach
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 3 p. 219 - 227
反应条件
1: With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate in acetonitrile T=130°C; Vorbrueggen glycosylation; 0.0833333 h; microwave irradiation; 2: With ammonia in methanol T=50°C; 16 h; Title compound not separated from byproducts;
参考文献
Bookser, Brett C.; Raffaele, Nicholas B.
Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 173 - 179
反应条件
1: SnCl4 / acetonitrile / 4 h / Ambient temperature 2: NH3 / methanol / 42 h / Ambient temperature View Scheme
参考文献
Baud; Chavis; Lucas; Imbach
Tetrahedron Letters, 1990 , vol. 31, # 31 p. 4437 - 4440
反应条件
1: HBr / CH2Cl2 / 3 h / -20 °C 2: liquid sulphur dioxide 3: 55 percent / NH3 / methanol / 72 h / -18 °C 4: 64 percent / Phosphoryl chloride, trimethyl phosphate / 4 h / 0 °C View Scheme
参考文献
Haynes et al.
Journal of the Chemical Society, 1957 , p. 3727,3731
反应条件
1: SnCl4 / acetonitrile / 20 °C 2: NH3 / methanol / 20 °C View Scheme
参考文献
Lioux, Thierry; Gosselin, Gilles; Mathe, Christophe
European Journal of Organic Chemistry, 2003 , # 20 p. 3997 - 4002
