alpha-甲基-1,3-苯并二氧代-5-乙醇合成路线 （共 14 条）
反应条件
1: 77 percent / NH4OAc / acetic acid / 5 h / Heating
2: 59 percent / Fe / FeCl3 / conc.HCl / H2O; ethanol / 8 h / Heating
3: 83.45 percent / NaBH4 / methanol / 16 h
View Scheme
参考文献
Bhide, Bhaskar H.; Shah, Kashmira K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 1 p. 9 - 12
反应条件
1: 59 percent / Fe / FeCl3 / conc.HCl / H2O; ethanol / 8 h / Heating
2: 83.45 percent / NaBH4 / methanol / 16 h
View Scheme
参考文献
Bhide, Bhaskar H.; Shah, Kashmira K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 1 p. 9 - 12
反应条件
NaBO3; borane
1.) THF, from 0 deg C to RT, 2 h, 2.) H2O, 25 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kabalka, George W.; Shoup, Timothy M.; Goudgaon, Naganna M.
Journal of Organic Chemistry, 1989 , vol. 54, # 25 p. 5930 - 5933
反应条件
1: 83.2 percent / HCl / diethyl ether; H2O / 3 h / 40 °C
2: CrO3 / acetic acid / 3 h / 60 °C
View Scheme
参考文献
Bhide, Bhaskar H.; Shah, Kashmira K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 1 p. 9 - 12
