反应条件
1.1: Br2BH-SMe2 / dichloromethane / 0 °C / Inert atmosphere
1.2: 0.25 h
2.1: pyridine; copper diacetate; sodium sulfate / 1,2-dichloro-ethane / 12 h / 25 °C
3.1: benzene-d6 / 12 h / 80 °C
4.1: silica gel / dichloromethane / 16 h / 25 °C
View Scheme
参考文献
Patil, Aditi S.; Mo, Dong-Liang; Wang, Heng-Yen; Mueller, Daniel S.; Anderson, Laura L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7799 - 7803
