2-羟基-5,8-二甲氧基-1,2,3,4-四氢萘合成路线 （共 9 条）
反应条件
oxalyl dichloride; dimethyl sulfoxide
参考文献
Manitto, Paolo; Speranza, Giovanna; Monti, Diego; Fontana, Gabriele; Panosetti, Elisa
Tetrahedron, 1995 , vol. 51, # 42 p. 11531 - 11546
反应条件
lithium aluminium tetrahydride in diethyl ether
5 h; Heating;
参考文献
Arvidsson; Hacksell; Johansson; Nilsson; Lindberg; Sanchez; Wikstroem; Svensson; Hjorth; Carlsson
Journal of Medicinal Chemistry, 1984 , vol. 27, # 1 p. 45 - 51
反应条件
1: 25 percent NH3 / dimethylsulfoxide / 10 h / 70 °C
2: hydrogen, NH3 / 10 percent Pd/C / methanol / 3 h / Ambient temperature
View Scheme
参考文献
Drandarov, Konstantin
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 5 p. 1111 - 1126
反应条件
1: 25 percent ammonia, 30 percent H2O2 / methanol / 20 h / Ambient temperature
2: 25 percent NH3 / dimethylsulfoxide / 10 h / 70 °C
3: hydrogen, NH3 / 10 percent Pd/C / methanol / 3 h / Ambient temperature
View Scheme
参考文献
Drandarov, Konstantin
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 5 p. 1111 - 1126
反应条件
sodium; benzene
anschliessendes Behandeln mit CH3I;
参考文献
Lewis et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5321,5322
反应条件
1: ethanol; charcoal
2: aq.-ethanolic HCl
3: sodium; benzene / anschliessendes Behandeln mit CH3I
View Scheme
参考文献
Lewis et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5321,5322
反应条件
1: ethanolic sodium ethylate / anschliessend mit CH3I
2: ethanol; charcoal
3: aq.-ethanolic HCl
4: sodium; benzene / anschliessendes Behandeln mit CH3I
View Scheme
参考文献
Lewis et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5321,5322
反应条件
1: aq.-ethanolic HCl
2: sodium; benzene / anschliessendes Behandeln mit CH3I
View Scheme
参考文献
Lewis et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5321,5322
反应条件
1: ethanol
2: ethanolic sodium ethylate / anschliessend mit CH3I
3: ethanol; charcoal
4: aq.-ethanolic HCl
5: sodium; benzene / anschliessendes Behandeln mit CH3I
View Scheme
参考文献
Lewis et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5321,5322
