4-甲氧基-3-吡咯啉-2-酮合成路线 （共 12 条）
反应条件
1.1: phosphorus oxytribromide / chloroform / 0.5 h / 0 °C
1.2: 6 h / 0 - 60 °C
2.1: palladium diacetate; triphenylphosphine / 1,4-dioxane; water; toluene / 70 °C / Inert atmosphere
2.2: 3 h / 100 °C / Inert atmosphere
3.1: hydrogenchloride; water / pH 7 / Inert atmosphere
View Scheme
参考文献
Dairi, Kenza; Yao, Yuxing; Faley, Michael; Tripathy, Sasmita; Rioux, Elise; Billot, Xavier; Rabouin, Daniel; Gonzalez, Gerson; Lavallee, Jean-Francois; Attardo, Giorgio
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 1051 - 1054
反应条件
1: methyl tetramate With n-butyllithium in tetrahydrofuran
T=-78°C;
2: allyl bromide in tetrahydrofuran
T=-78°C;
参考文献
Hunter, Roger; Richards, Philip
Synlett, 2003 , # 2 p. 271 - 273
