4-氯-N,N-二甲基苯胺合成路线 （共 152 条）
反应条件
1: bromobenzene With lithium in diethyl ether
2: With zinc(II) chloride in tetrahydrofuran; diethyl ether
T=20°C; 1 h;
3: 4-Me2NC6H4Cl With nickel phosphine amido pincer complex in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=70°C; 3 h; Further stages.;
参考文献
Wang, Li; Wang, Zhong-Xia
Organic Letters, 2007 , vol. 9, # 21 p. 4335 - 4338
反应条件
triphenyl phosphite; K3PO4*3H2O; Ipr.HCl; palladium diacetate in tert-butyl alcohol
T=80°C; 10 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
反应条件
in acetonitrile
Irradiation;
参考文献
Fagnoni, Maurizio; Mella, Mariella; Albini, Angelo
Organic Letters, 1999 , vol. 1, # 8 p. 1299 - 1301
反应条件
triethylamine in acetonitrile
16 h; Irradiation;
参考文献
Dichiarante, Valentina; Betti, Cecilia; Fagnoni, Maurizio; Maia, Angelamaria; Landini, Dario; Albini, Angelo
Chemistry - A European Journal, 2007 , vol. 13, # 6 p. 1834 - 1841
反应条件
in acetonitrile
1 h; Irradiation;
参考文献
Guizzardi; Mella; Fagnoni; Freccero; Albini
Journal of Organic Chemistry, 2001 , vol. 66, # 19 p. 6353 - 6363
反应条件
cerium (IV) sulfate; sodium nitrite in water
T=20°C; 1 h;
参考文献
Yang, Xianghua; Xi, Chanjuan
Synthetic Communications, 2007 , vol. 37, # 19 p. 3381 - 3392
反应条件
acetic acid; sodium nitrite
T=21°C; 1.5 h; other N,N-dialkyl aromatic amines; other solvent, var. times, also with addition gases (N2, NO, O2); deuterium kinetics isotope effect; Product distributionMechanism;
参考文献
Loeppky, Richard N.; Singh, Sukhjeet P.; Elomari, Saleh; Hastings, Riley; Theiss, Thomas E.
Journal of the American Chemical Society, 1998 , vol. 120, # 21 p. 5193 - 5202
参考文献
Clemo; Smith
Journal of the Chemical Society, 1928 , p. 2420
参考文献
Clemo; Smith
Journal of the Chemical Society, 1928 , p. 2420
参考文献
Clemo; Smith
Journal of the Chemical Society, 1928 , p. 2420
