4-氯-N,N-二甲基苯胺合成路线 (共 152 条)
反应条件
palladium diacetate in acetic acid; benzene
Yield given. Yields of byproduct given;
参考文献
Sakakibara, Tsutomu; Hamakawa, Tomoko
Chemistry Letters, 1982 , p. 1823 - 1824
反应条件
C36H45Cl2N3OPd; potassium tert-butylate in 1,4-dioxane
T=90°C; Buchwald-Hartwig Coupling; 1 h; Inert atmosphereSchlenk technique;
参考文献
Huang, Pei; Wang, Yi-Xiang; Yu, Hong-Fei; Lu, Jian-Mei
Organometallics, 2014 , vol. 33, # 7 p. 1587 - 1593
反应条件
in acetonitrile
Irradiation;
参考文献
Fagnoni, Maurizio; Mella, Mariella; Albini, Angelo
Organic Letters, 1999 , vol. 1, # 8 p. 1299 - 1301
反应条件
in acetonitrile
ionic Meerwein arylation; Irradiation;
参考文献
Mella; Coppo; Guizzardi; Fagnoni; Freccero; Albini
Journal of Organic Chemistry, 2001 , vol. 66, # 19 p. 6344 - 6352
反应条件
in dimethyl sulfoxide
T=20°C; 10 h; UV-irradiation; Product distribution; Further Variations:Solvents;
参考文献
Ito, Yoshikatsu
Tetrahedron, 2007 , vol. 63, # 15 p. 3108 - 3114
反应条件
triethylamine in acetonitrile
5 h; Irradiation;
参考文献
Fraboni, Andrea; Fagnoni, Maurizio; Albini, Angelo
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4886 - 4893
反应条件
N-ethyl-N,N-diisopropylamine in toluene
Heating;
参考文献
Cheng; Zhan; Meth-Cohn
Synthesis, 2002 , # 1 p. 34 - 38
反应条件
in benzene
48 h; Ambient temperature;
参考文献
Miyagi, Yo; Maruyama, Kazuhiro; Kurokawa, Mitsunori; Yoshii, Ayumi
Chemistry Letters, 1988 , p. 51 - 54
反应条件
sulfuric acid; chlorine; silver sulphate
参考文献
Gorvin
Journal of the Chemical Society, 1953 , p. 1237,1241
反应条件
in benzene
48 h; Ambient temperature;
参考文献
Miyagi, Yo; Maruyama, Kazuhiro; Kurokawa, Mitsunori; Yoshii, Ayumi
Chemistry Letters, 1988 , p. 51 - 54