4-氯-N,N-二甲基苯胺合成路线 (共 152 条)
反应条件
1: 2-methyl-propan-2-ol; H2O / 5.5 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W)
2: KOH / H2O / 0.33 h / Heating
3: air / H2O / 3 h / Ambient temperature
View Scheme
参考文献
Frolov, A. N.; Klokova, E. M.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2161 - 2170
反应条件
in dimethyl sulfoxide
T=20°C; 10 h; UV-irradiation; Product distribution; Further Variations:Solvents;
参考文献
Ito, Yoshikatsu
Tetrahedron, 2007 , vol. 63, # 15 p. 3108 - 3114