4-氯-N,N-二甲基苯胺合成路线 (共 152 条)
反应条件
(ethyl)-triphenylphosphonium iodide T=170°C; 1.25 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 71, # 15 p. 5770 - 5773
反应条件
formic acid; triethylamine T=150°C; 12 h; Inert atmosphereGreen chemistry;
参考文献
Chemistry - A European Journal, , vol. 20, # 1 p. 58 - 63
反应条件
formic acid; iron(II) chloride heptahydrate; triethylamine T=150°C; 12 h;
参考文献
Chemistry - A European Journal, , vol. 20, # 1 p. 58 - 63
反应条件
in chloroform T=5°C; 3 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 42, # 9 p. 1760 - 1767
反应条件
1H-imidazole; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in chloroform T=25°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 27, # 14 p. 1617 - 1620
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Synthetic Communications, , vol. 40, # 20 p. 3078 - 3083
反应条件
hydrogen in hexane T=160°C; 48 h; Autoclave;
参考文献
Chemical Science, , vol. 5, # 2 p. 649 - 655
参考文献
Journal of the Chemical Society, , p. 1199
反应条件
N-chlorotriethylammonium chloride in trifluoroacetic acid Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 385 - 392
反应条件
iron(III) chloride T=20°C; 168 h; Further byproducts given;
参考文献
Canadian Journal of Chemistry, , vol. 83, # 3 p. 244 - 250