4-氯-N,N-二甲基苯胺合成路线 (共 152 条)
反应条件
titanium tetrachloride in dichloromethane T=0 - 25°C; N-dealkylation; 8 h;
参考文献
Periasamy, Mariappan; Jayakumar, K. Natarajan; Bharathi, Pandi
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3548 - 3550
反应条件
Mn(NO3)2; oxygen in acetonitrile T=50°C; 20 h; Yields of byproduct given;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Heterocycles, 1993 , vol. 36, # 9 p. 2147 - 2153
反应条件
{Ru(IV)O(2,2`-bipyridine)(PPh3)}(ClO4)2 in acetonitrile T=21°C; other Ru(IV) complex catalyst, ΔH(excit), ΔS(excit) determined; Rate constantKineticsThermodynamic data;
参考文献
Leising, Randolph A.; Ohman, Jeffrey S.; Acquaye, John H.; Takeuchi Kenneth J.
Journal of the Chemical Society, Chemical Communications, 1989 , # 14 p. 905 - 906
反应条件
Mn(NO3)2; oxygen in acetonitrile T=50°C; 20 h; Yields of byproduct given;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Heterocycles, 1993 , vol. 36, # 9 p. 2147 - 2153
反应条件
Benzoyl cyanide; oxygen; iron(III) chloride in acetonitrile T=50°C; P=760 Torr; 16 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1297 - 1298
反应条件
oxygen; iron(III) chloride in acetonitrile T=50°C; P=760 Torr; 16 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1297 - 1298
反应条件
palladium diacetate; acetic acid in benzene T=80°C; 5 h;
参考文献
Chemistry Letters, , p. 1331 - 1334
反应条件
oxygen; acetic anhydride in acetonitrile T=30°C; 10 h;
参考文献
Chemistry Letters, , # 5 p. 757 - 760
反应条件
in dichloromethane Kinetics; mixing (223 K); not isolated; UV-VIS spectroscopy (413 nm);
参考文献
Goto; Watanabe; Fukuzumi; Jones; Dinnocenzo
Journal of the American Chemical Society, 1998 , vol. 120, # 41 p. 10762 - 10763
反应条件
in acetonitrile Kinetics; byproducts: CH2O; stoicheiometric oxidation of 4-chloro-N,N-dimethylaniline by the Ru complex in MeCN at 21°C; spectrophotometrical determination of the rate constant;
参考文献
Leising, Randolph A.; Ohman, Jeffrey S.; Acquaye, John H.; Takeuchi Kenneth J.
Journal of the Chemical Society, Chemical Communications, 1989 , # 14 p. 905 - 906