4-氯-N,N-二甲基苯胺合成路线 (共 152 条)
反应条件
in acetonitrile Kinetics; byproducts: CH2O; stoicheiometric oxidation of 4-chloro-N,N-dimethylaniline by the Ru complex in MeCN at 21°C; spectrophotometrical determination of the rate constant;
参考文献
Leising, Randolph A.; Ohman, Jeffrey S.; Acquaye, John H.; Takeuchi Kenneth J.
Journal of the Chemical Society, Chemical Communications, 1989 , # 14 p. 905 - 906
反应条件
oxygen in acetonitrile T=30°C; P=760 Torr; 10 h; other temperature, other 4-substituted N,N-dialkylanilines; Product distribution;
参考文献
Chemistry Letters, , # 5 p. 757 - 760
反应条件
dihydrogen peroxide; oxygen; iron(II) sulfate in sulfuric acid; water Ambient temperaturepH=2; further objects: pH-dependence (1.8), different substrate concentrations; Product distributionMechanism;
参考文献
Gazzetta Chimica Italiana, , vol. 113, # 3/4 p. 207 - 212
反应条件
1,4-diaza-bicyclo[2.2.2]octane in chloroform Friedel-Crafts acylation; 22 h; Heating;
参考文献
Synthesis, , # 6 p. 904 - 908
反应条件
air in chloroform Cyclization; 18 h; Heating;
参考文献
Tetrahedron Letters, , vol. 41, # 18 p. 3475 - 3478
反应条件
in water; tert-butyl alcohol T=20 - 21°C; flash photolysis; Product distributionRate constantMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 856 - 861
Zhurnal Organicheskoi Khimii, , vol. 19, # 5 p. 966 - 972
反应条件
acetic acid; sodium nitrite T=21°C; 1.5 h; other N,N-dialkyl aromatic amines; other solvent, var. times, also with addition gases (N2, NO, O2); deuterium kinetics isotope effect; Product distributionMechanism;
参考文献
Tanno; Sueyoshi; Miyata
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 9 p. 1760 - 1767
参考文献
Schmidt; Fischer
Chemische Berichte, 1920 , vol. 53, p. 1539
参考文献
Schmidt; Fischer
Chemische Berichte, 1920 , vol. 53, p. 1539
反应条件
1: H2SO4; NaNO2 2: tin; hydrochloric acid View Scheme
参考文献
Pinnow
Chemische Berichte, 1898 , vol. 31, p. 2984