Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
1: 88 percent / TsOH / benzene / 24 h / Heating
2: 1.) BuLi / 1.) THF, -78 deg C, 10 min, 2.) -78 deg C -> room temperature
3: 74 percent / NaH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
1: 88 percent / TsOH / benzene / 24 h / Heating
2: 1.) BuLi / 1.) THF, -78 deg C, 10 min, 2.) -78 deg C -> room temperature
3: 83 percent / NaH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902