Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
1: Na2CO3, MCPBA / CH2Cl2 / 96 h / Ambient temperature
2: 92 percent / TFA / 2 h / 34 °C
View Scheme
参考文献
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
1: TFA / 1 h / Heating
2: Na2CO3, MCPBA / CH2Cl2 / 96 h / Ambient temperature
3: 92 percent / TFA / 2 h / 34 °C
View Scheme
参考文献
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) 5 min
2: TFA / 1 h / Heating
3: Na2CO3, MCPBA / CH2Cl2 / 96 h / Ambient temperature
4: 92 percent / TFA / 2 h / 34 °C
View Scheme
参考文献
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892