Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
sodium hydride in tetrahydrofuran
1 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
sodium hydride in tetrahydrofuran
20 h; Ambient temperature;
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
1: 91 percent / TsOH / benzene / Heating
2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min
3: 24 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature
View Scheme
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min
2: 24 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature
View Scheme
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min
2: 76 percent / NaH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min, 2.) 10 min
2: 96 percent / NaH / tetrahydrofuran / 0.5 h / Ambient temperature
3: 85 percent / aq. H2SO4 / tetrahydrofuran / 48 h
View Scheme
参考文献
Earnshaw, Chris; Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2893 - 2902
