hydrogen; Pd on polytris(hydroxymethyl)melamine in ethanol T=45°C; P=757.6 Torr; 1 h; activation energy, other catalysts: Pd/C, palladium on aminated and chloromethylated styrene-divinylbenzene copolymer anion exchange resin AV-17-8 matrix, other solvents: 1-propanol, 2-propanol, 1-butanol, 2-methyl-2-propanol, toluene, hexane; Rate constantKinetics;

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in toluene 1.) 0 deg C, 1 h; 2.) room temperature, overnight;

1: NaBH4 / ethanol 2: 90 percent / benzene / 25 °C 3: 37 percent / phosphoric acid / 1 h / 70 - 100 °C View Scheme