(4-甲氧基苯基)-1-吡咯烷甲酮合成路线 (共 17 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Heating;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
mercury dibromide in toluene
12 h; Heating;
参考文献
Fujiwara, Shin-Ichi; Ogawa, Akiya; Kambe, Nobuaki; Ryu, Ilhyong; Sonoda, Noboru
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6121 - 6124
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
T=60°C; P=750.075 Torr; 14 h; Microreactor; chemoselective reaction;
参考文献
De La Fuente, Veronica; Godard, Cyril; Zangrando, Ennio; Claver, Carmen; Castillon, Sergio
Chemical Communications, 2012 , vol. 48, # 11 p. 1695 - 1697
反应条件
1: SOCl2 / 2 h / 80 °C
2: CH2Cl2 / 20 °C
View Scheme
参考文献
Karimi, Farhad; Langstroem, Bengt
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 3 p. 541 - 546
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Heating;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
1: 70 - 75 °C
2: dihydrogen peroxide / 2 h / 70 - 75 °C
View Scheme
参考文献
Tank, Rekha; Pathak, Uma; Vimal, Manorama; Bhattacharyya, Shubhankar; Pandey, Lokesh Kumar
Green Chemistry, 2011 , vol. 13, # 12 p. 3350 - 3354
反应条件
boron tribromide in dichloromethane
T=20°C; demethylation; 72 h;
参考文献
Sasse; Sadek; Ligneau; Elz; Pertz; Luger; Ganellin; Arrang; Schwartz; Schunack; Stark
Journal of Medicinal Chemistry, 2000 , vol. 43, # 17 p. 3335 - 3343