2-(4-甲基苯基)乙醇合成路线 (共 73 条)
反应条件
potassium hydroxide T=215°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 5, p. 555,560
Chem. Zentralbl., , vol. 106, # II p. 3081
反应条件
phosphorus tribromide T=0 - 100°C; 17 h;
参考文献
Burke, Christopher P.; Shi, Yian
Organic Letters, 2009 , vol. 11, # 22 p. 5150 - 5153
反应条件
ruthenium trichloride; (NH4)2Ce(NO3)2; nitric acid in acetonitrile T=24.85°C; Kinetics;
参考文献
Rao, N. Vijaya Bhaskar; Rao, M. Anand
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2005 , vol. 44, # 1 p. 80 - 84
反应条件
1: With N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 2.5 h; Inert atmosphere; 2: With trimethylsilyl trifluoromethanesulfonate in acetonitrile T=0 - 20°C;
参考文献
Liu, Xigong; Sun, Bin; Xie, Zhiyu; Qin, Xiaojun; Liu, Lei; Lou, Hongxiang
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3104 - 3112
反应条件
1: ethyldiisopropylamine / CH2Cl2 / 24 h / 20 °C 2: TiCl4 / CH2Cl2 / 6 h / -40 °C View Scheme
参考文献
Szymanska, Ewa; Frydenvang, Karla; Contreras-Sanz, Alberto; Pickering, Darryl S.; Frola, Elena; Serafimoska, Zorica; Nielsen, Birgitte; Kastrup, Jette S.; Johansen, Tommy N.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 20 p. 7289 - 7298
参考文献
Schmitz
Chemische Berichte, 1958 , vol. 91, p. 1133,1138
反应条件
1: hydrogen chloride 2: bromine; tetrachloromethane / Irradiation.mit UV-Licht, Erw. des auf 130grad erh. Rktprod. mit wss. Bromwasserstoffsaeure u. Beh. des erh. 2-<2-Brom-aethyl>-5-methyl-benzaldehyds mit Ammoniak enth. Methanol View Scheme
参考文献
Chemische Berichte, , vol. 91, p. 1133,1138
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile T=80°C; 2 h;
参考文献
Revelant, Germain; Dunand, Sandrine; Hesse, Stephanie; Kirsch, Gilbert
Synthesis, 2011 , # 18 art. no. Z45811SS, p. 2935 - 2940
反应条件
(i) SOCl2, benzene, (ii) N2H4*H2O, nPrOH; Multistep reaction;
参考文献
Bream,J.B. et al.
Journal of Medicinal Chemistry, 1970 , vol. 13, # 6 p. 1051 - 1057
反应条件
thionyl chloride; N,N-dimethyl-aniline
参考文献
Ichii,M.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, # 9 p. 2810 - 2813