反应条件
1: With chloro-trimethyl-silane; ethylene dibromide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; lithium chloride; cobalt(II) chloride; zinc in tetrahydrofuran
T=20°C; 14 h; Inert atmosphereSchlenk technique;
2: With trimethylsilyl-methylmagnesium chloride in tetrahydrofuran
T=0°C; 1 h; Inert atmosphereSchlenk technique;
参考文献
Tan, Boon-Hong; Dong, Jinghua; Yoshikai, Naohiko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 38 p. 9610 - 9614
