1: 1-bromospiro[5.5]undec-1-ene With tert.-butyl lithium in tetrahydrofuran; hexane
T=-80°C; Inert atmosphere;
2: methyl vinyl ketone in tetrahydrofuran; hexane
T=-80 - 20°C; Inert atmosphere;
3: With water in tetrahydrofuran; hexane
T=20°C;
参考文献
Asachenko, Andrey F.; Kononovich, Dmitry S.; Zharov, Andrey N.; Razavi, Abbas; Voskoboynikov, Alexander Z.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 15-16 p. 1940 - 1948
