1-(2-溴苯基)-1H-吡咯合成路线 (共 6 条)
反应条件
ionic liquid immobilized on γ-Fe2O3(at)SiO2 nanoparticles in water T=100°C; Clauson-Kaas Synthesis; 1.5 h;
参考文献
Ma, Fei-Ping; Li, Pei-He; Li, Bao-Le; Mo, Li-Ping; Liu, Ning; Kang, Hui-Jun; Liu, Ya-Nan; Zhang, Zhan-Hui
Applied Catalysis A: General, 2013 , vol. 457, p. 34 - 41
反应条件
copper; caesium carbonate in acetonitrile 12 h; RefluxInert atmosphere; chemoselective reaction;
参考文献
Zhu, Rui; Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Su, Deyong; Hu, Yuefei
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 9 p. 1253 - 1257
反应条件
Suzuki-Miyaura coupling;
参考文献
Journal of Organic Chemistry, , vol. 75, # 14 p. 4835 - 4840
反应条件
caesium carbonate; palladium diacetate; triphenylphosphine in toluene T=120°C;
参考文献
Hulcoop, David G.; Lautens, Mark
Organic Letters, 2007 , vol. 9, # 9 p. 1761 - 1764
反应条件
1: CuI; Et3N / PdCl2(PPh3)2 / dimethylformamide / 16 h / Heating 2: K2CO3 / methanol / 1 h / 20 °C 3: 56 percent / PtCl2 / toluene / 30 h / 80 °C View Scheme
参考文献
Fuerstner, Alois; Mamane, Victor
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6264 - 6267
反应条件
1: POCl3
2: 93 percent / sodium hydroxide, silver oxide / ethanol / 23 h / Ambient temperature
3: 13 percent / n-BuLi / tetrahydrofuran; hexane / 2 h / -100 - -20 °C
View Scheme
参考文献
Cartoon, M. E. K.; Cheeseman, G. W. H.
Journal of Organometallic Chemistry, 1981 , vol. 212, # 1 p. 1 - 9