N-(1-氧化吡啶-2-基)乙酰胺合成路线 (共 7 条)
反应条件
1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate; triethylamine in acetonitrile T=150°C; 1 h; Microwave irradiation; chemoselective reaction;
参考文献
Fuentes, Jose A.; Clarke, Matthew L.
Synlett, 2008 , # 17 p. 2579 - 2582
参考文献
Adams; Miyano
Journal of the American Chemical Society, 1954 , vol. 76, p. 2785
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C;
参考文献
Clarke, Matthew L.; Fuentes, Jose A.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 6 p. 930 - 933
反应条件
1: 2 h / 80 °C
2: m-chloroperbenzoic acid / CH2Cl2 / 20 °C
View Scheme
参考文献
Clarke, Matthew L.; Fuentes, Jose A.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 6 p. 930 - 933
参考文献
Adams; Miyano
Journal of the American Chemical Society, 1954 , vol. 76, p. 2785
反应条件
1: acetic acid; aqueous H2O2 / Erhitzen mit konz. wss. HCl und Behandeln mit aethanol. Natriumaethylat
2: acetonitrile
View Scheme
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197