双(4-甲氧基苯基)二甲基硅烷合成路线 (共 3 条)
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether
T=-15°C; 1 h;
2: dimethyl-dichlorosilane in diethyl ether
参考文献
Van Der Vlugt, Jarl Ivar; Bonet, Josep M.; Mills, Allison M.; Spek, Anthony L.; Vogt, Dieter
Tetrahedron Letters, 2003 , vol. 44, # 23 p. 4389 - 4392
反应条件
in diethyl ether
5 h; Ambient temperature;
参考文献
Walree, Cornelis A. van; Lauteslager, Xavier Y.; Wageningen, Andreas M. A. van; Zwikker, Jan W.; Jenneskens, Leonardus W.
Journal of Organometallic Chemistry, 1995 , vol. 496, # 1 p. 117 - 126
反应条件
in diethyl ether
Alkylation; 1 h; Heating; Title compound not separated from byproducts.;
参考文献
Studer, Armido; Bossart, Martin; Vasella, Tomaso
Organic Letters, 2000 , vol. 2, # 7 p. 985 - 988