1: toluene-4-sulfonamide With sodium hydride in N,N-dimethyl-formamide; mineral oil T=65°C; 1 h; Inert atmosphere; 2: 1,2-bis-(bromomethyl)benzene in N,N-dimethyl-formamide; mineral oil T=65°C; 3 h; Inert atmosphere;
参考文献
Anastasiadis, Charalampos; Hogarth, Graeme; Wilton-Ely, James D.E.T.
Inorganica Chimica Acta, 2010 , vol. 363, # 13 p. 3222 - 3228
sodium hydride; N,N-dimethyl-formamide anschliessendes Behandeln mit α,α'-Dibrom-o-xylol;
参考文献
Bornstein et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1255
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Bornstein; Shields
Organic Syntheses, 1973 , vol. Coll. Vol. V, p. 1064
