腺嘌呤N(1)-氧化物单水合物合成路线 （共 5 条）
反应条件
1: 66.2 percent / aq. NaNO2, aq. HOAc / H2O / 2 h / 70 - 80 °C 2: 39.9 percent / POCl3, NEt3 / 3 h / Heating 3: 80.5 percent / butan-1-ol / 5 h / 100 °C View Scheme
参考文献
Oh, Chang-Hyun; Lee, Su-Chul; Lee, Ki-Soo; Woo, Eun-Rhan; Hong, Chang Yong; Yang, Boem-Seok; Baek, Dae Jin; Cho, Jung-Hyuck
Archiv der Pharmazie, 1999 , vol. 332, # 6 p. 187 - 190
反应条件
1: 66.2 percent / aq. NaNO2, aq. HOAc / H2O / 2 h / 70 - 80 °C 2: 39.9 percent / POCl3, NEt3 / 3 h / Heating 3: 80.5 percent / butan-1-ol / 5 h / 100 °C 4: NaH / dimethylformamide / 20 °C View Scheme
参考文献
Oh, Chang-Hyun; Lee, Su-Chul; Lee, Ki-Soo; Woo, Eun-Rhan; Hong, Chang Yong; Yang, Boem-Seok; Baek, Dae Jin; Cho, Jung-Hyuck
Archiv der Pharmazie, 1999 , vol. 332, # 6 p. 187 - 190
反应条件
1: 66.2 percent / aq. NaNO2, aq. HOAc / H2O / 2 h / 70 - 80 °C 2: 39.9 percent / POCl3, NEt3 / 3 h / Heating View Scheme
参考文献
Oh, Chang-Hyun; Lee, Su-Chul; Lee, Ki-Soo; Woo, Eun-Rhan; Hong, Chang Yong; Yang, Boem-Seok; Baek, Dae Jin; Cho, Jung-Hyuck
Archiv der Pharmazie, 1999 , vol. 332, # 6 p. 187 - 190
反应条件
1: 66.2 percent / aq. NaNO2, aq. HOAc / H2O / 2 h / 70 - 80 °C 2: 39.9 percent / POCl3, NEt3 / 3 h / Heating 3: 80.5 percent / butan-1-ol / 5 h / 100 °C 4: 90.5 percent / NaH / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Oh, Chang-Hyun; Lee, Su-Chul; Lee, Ki-Soo; Woo, Eun-Rhan; Hong, Chang Yong; Yang, Boem-Seok; Baek, Dae Jin; Cho, Jung-Hyuck
Archiv der Pharmazie, 1999 , vol. 332, # 6 p. 187 - 190
反应条件
acetic acid; sodium nitrite in water
T=70 - 80°C; 2 h;
参考文献
Oh, Chang-Hyun; Lee, Su-Chul; Lee, Ki-Soo; Woo, Eun-Rhan; Hong, Chang Yong; Yang, Boem-Seok; Baek, Dae Jin; Cho, Jung-Hyuck
Archiv der Pharmazie, 1999 , vol. 332, # 6 p. 187 - 190
