(6CI,7CI,8CI,9CI)-4-甲基喹唑啉合成路线 （共 35 条）
反应条件
1: 50percent sodium hydride in oil dispersion / dimethylformamide / 3 h
2: 40percent potassium hydroxide / ethanol; H2O / Heating
View Scheme
参考文献
Kant, Joydeep; Popp, Frank D.; Uff, Barrie C.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1313 - 1316
反应条件
1: diethyl ether
2: aqueous NaOH; methanol. KOH
View Scheme
参考文献
Elderfield; Serlin
Journal of Organic Chemistry, 1951 , vol. 16, p. 1669,1680
参考文献
Elderfield; Serlin
Journal of Organic Chemistry, 1951 , vol. 16, p. 1669,1680
反应条件
1: 47 percent / PdCl2(PPh3)2, MoCl5, CO / 16 h / 120 °C / 14710.2 Torr
2: 44 percent / PdCl2(PPh3)2, MoCl5, CO / 16 h / 120 °C / 14710.2 Torr
View Scheme
参考文献
Akazome, Motohiro; Yamamoto, Jun; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1995 , vol. 494, # 12 p. 229 - 234
反应条件
1: PdCl2(PPh3)2, MoCl5, CO / 16 h / 120 °C / 14710.2 Torr / other substituted aromatic ketones; other reagents; var. temp. and time
2: 44 percent / PdCl2(PPh3)2, MoCl5, CO / 16 h / 120 °C / 14710.2 Torr
View Scheme
参考文献
Akazome, Motohiro; Yamamoto, Jun; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1995 , vol. 494, # 12 p. 229 - 234
反应条件
1: 72 percent / sodium hydride, DMF / 3 h / Ambient temperature
2: 9 percent / benzoic acid / Heating; base hydrolysis, various reagents
View Scheme
参考文献
Hahn, Jung-Tai; Popp, Frank D.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1357 - 1372
反应条件
in acetonitrile
T=20°C; 1 h; Inert atmosphereUV-irradiation; Quantum yield;
参考文献
Alonso, Rafael; Caballero, Alegria; Campos, Pedro J.; Sampedro, Diego; Rodriguez, Miguel A.
Tetrahedron, 2010 , vol. 66, # 25 p. 4469 - 4473
反应条件
potassium hydroxide; water in ethanol
3.5 h; Heatingfurther reagent;
参考文献
Hahn, Jung-Tai; Popp, Frank D.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1357 - 1372
参考文献
Bogert; Nabenhauer
Journal of the American Chemical Society, 1924 , vol. 46, p. 1705,1933
参考文献
Adachi
Yakugaku Zasshi, 1957 , vol. 77, p. 507,510
Chem.Abstr., 1957 , p. 14744
