5-苯基-3,4-二氢-2H-吡咯合成路线 (共 67 条)
反应条件
copper(I)-thiophene-2-carboxylate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=100°C; P=1500.15 - 2250.23 Torr; 1 h; microwave irradiation;
参考文献
Prokopcova, Hana; Kappe, C. Oliver
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 3 p. 448 - 452
反应条件
triethyl phosphite in dimethyl sulfoxide
0.133333 h; microwave irradiation;
参考文献
Singh, Pradeep N.D.; Klima, Rodney F.; Muthukrishnan, Sivaramakrishnan; Murthy, Rajesh S.; Sankaranarayanan, Jagadis; Stahlecker, Heidi M.; Patel, Bhavika; Gudmundsdottir, Anna D.
Tetrahedron Letters, 2005 , vol. 46, # 24 p. 4213 - 4217
反应条件
3,3-dimethylbut-1-ene; RhCl(CO)(PFur3)2; caesium carbonate in 1,4-dioxane
T=120°C; 10 h;
参考文献
Sezen, Bengue; Sames, Dalibor
Journal of the American Chemical Society, 2004 , vol. 126, # 41 p. 13244 - 13246
反应条件
in dichloromethane
T=20°C; 48 h;
参考文献
Sun, Xiaowei; Gao, Chengzhe; Zhang, Fan; Song, Zhuang; Kong, Lingyi; Wen, Xiaoan; Sun, Hongbin
Tetrahedron, 2014 , vol. 70, # 3 p. 643 - 649
反应条件
sodium azide; triethyl phosphite in dimethyl sulfoxide
intramolecular aza-Wittig reaction; 0.333333 h; microwave irradiation;
参考文献
Singh, Pradeep N.D.; Klima, Rodney F.; Muthukrishnan, Sivaramakrishnan; Murthy, Rajesh S.; Sankaranarayanan, Jagadis; Stahlecker, Heidi M.; Patel, Bhavika; Gudmundsdottir, Anna D.
Tetrahedron Letters, 2005 , vol. 46, # 24 p. 4213 - 4217
反应条件
zirconium triflate; toluene-4-sulfonamide in 1,2-dichloro-ethane
T=60°C; 48 h;
参考文献
Shi, Min; Yang, Yong-Hua; Xu, Bo
Synlett, 2004 , # 9 p. 1622 - 1624
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in toluene
T=20°C; 0.5 h;
参考文献
Mans, Douglas M.; Pearson, William H.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6419 - 6426
反应条件
water; lithium chloride in dimethyl sulfoxide
T=140 - 150°C; 3 h;
参考文献
More, Satish S.; Mohan, T. Krishna; Kumar, Y. Sateesh; Kumar, U.K. Syam; Patel, Navin B.
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 831 - 838
反应条件
1: pyrrolidin-2-one With chloro-trimethyl-silane; triethylamine in diethyl ether
0.5 h; Heating;
2: Bromure de phenyl magnesium in diethyl ether
3 h; Heating;
参考文献
Coindet, Cecile; Comel, Alain; Kirsch, Gilbert
Tetrahedron Letters, 2001 , vol. 42, # 35 p. 6101 - 6104
反应条件
Ru(H)2(CO)(PCy3)3 in tert-butyl alcohol
T=150°C;
参考文献
Sezen, Bengue; Sames, Dalibor
Journal of the American Chemical Society, 2005 , vol. 127, # 15 p. 5284 - 5285