5-苯基-3,4-二氢-2H-吡咯合成路线 （共 67 条）
反应条件
Irradiationinvestigation of photocyclization (diradical) and fluoride ion induced (dipolar) reactions; Product distributionQuantum yieldMechanism;
参考文献
Lan,A.J.; Heukeroth,R.O.; Mariano,P.S.
Journal of the American Chemical Society, 1987 , vol. 109, p. 2738
反应条件
1: 79 percent / NiCl2, NaBH4 / methanol / 14 h / -30 - 20 °C
2: 64 percent / 4-(dimethylamino)pyridine, NEt3 / CH2Cl2 / 16 h / Ambient temperature
View Scheme
参考文献
Karl Dieter; Li, ShengJian
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7726 - 7735
反应条件
1: acetonitrile / 8 h / Ambient temperature
2: 48 percent / 1.) 1 N aq. NaOH / 1.) ether, ice-cooling, 0.5 h, 2.) room temp., 8 h
View Scheme
参考文献
Dannhardt; Obergrusberger
Archiv der Pharmazie, 1981 , vol. 314, # 9 p. 787 - 798
反应条件
in ethylene glycol dimethyl ether; diethyl ether
参考文献
Dannhardt; Obergrusberger
Archiv der Pharmazie, 1984 , vol. 317, # 2 p. 143 - 151
反应条件
in ethylene glycol dimethyl ether; diethyl ether
参考文献
Dannhardt; Obergrusberger
Archiv der Pharmazie, 1984 , vol. 317, # 2 p. 143 - 151
反应条件
1: 17 percent / 1,2-dimethoxy-ethane / 48 h / Ambient temperature
2: 73 percent / 2 N NaOH / dioxane / 6 h / Heating
View Scheme
参考文献
Dannhardt; Obergrusberger
Archiv der Pharmazie, 1984 , vol. 317, # 2 p. 143 - 151
反应条件
1: 59 percent / 1,2-dimethoxy-ethane; diethyl ether
2: 81 percent / 2 N NaOH / 0.5 h / 80 °C
View Scheme
参考文献
Dannhardt; Obergrusberger
Archiv der Pharmazie, 1984 , vol. 317, # 2 p. 143 - 151
