(R)-(+)-1,2,4-丁三醇合成路线 (共 23 条)
反应条件
boric acid trimethyl ester; dimethylsulfide borane complex in tetrahydrofuran Inert atmosphere;
参考文献
Williams, David R.; Plummer, Scott V.; Patnaik, Samarjit
Tetrahedron, 2011 , vol. 67, # 27-28 p. 5083 - 5097
反应条件
sodium borohydride in tetrahydrofuran; methanol
参考文献
Avecia Limited
Patent: US6479714 B1, 2002 ;
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; P=750.075 Torr;
参考文献
Andersen, Nikolaj Rojkjaaer; Hansen, Signe Grann; Bertelsen, Soren; Jorgensen, Karl Anker
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 18 p. 3193 - 3198
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
indium trifluoromethanesulfonate in tetrahydrofuran; water T=100°C; 0.0833333 h; Microwave irradiation;
参考文献
Golden, Kathryn C.; Gregg, Brian T.; Quinn, John F.
Tetrahedron Letters, 2010 , vol. 51, # 31 p. 4010 - 4013
反应条件
1: With L-arabinose dehydrogenase from P. fragi ATCC 4973 T=30°C; pH=6.4; 2: With potassium hydroxide T=20°C; pH=12.0; 3: With E. coli BL21(DE3); pWN6.222A in water T=33°C; ambient pressure;
参考文献
Journal of the American Chemical Society, , vol. 125, # 43 p. 12998 - 12999
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium hydroxide; PEP; adenosine 5'-triphosphoric acid; magnesium chloride in water T=27°C; 216 h; pH=7.5; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 107, # 24 p. 7019 - 7027