(R)-(+)-1,2,4-丁三醇合成路线 （共 23 条）
反应条件
Raney Ni(W-2) in ethanol 5 h; Heating;
参考文献
Yamada; Ogasawara
Synthesis, 1995 , # 10 p. 1291 - 1294
反应条件
(R,R)-N-lt;3,5-di-t-butyl-6-(11-(silica-O-SiMe2-linked)undecyloxy)gt;benzylidene-N'-(3-t-butyl-2,5-dihydroxy)benzylidene-1,2-cyclohexanediamine - (acetoxy)Co; water in tetrahydrofuran Ambient temperature; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 121, # 17 p. 4147 - 4154
反应条件
hydrogen; palladium on activated charcoal in methanol 5 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 45, # 5 p. 1501 - 1508
反应条件
toluene-4-sulfonic acid in methanol
参考文献
Tetrahedron, , vol. 35, p. 933 - 940
反应条件
sodium tetrahydroborate in methanol Ambient temperature; Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 13 p. 1631 - 1636
反应条件
sodium tetrahydroborate
参考文献
Tetrahedron Letters, , vol. 31, # 29 p. 4147 - 4150
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 52, # 11 p. 2137 - 2141
反应条件
sodium hydroxide; sodium azide; pyruvate kinase; Phosphoenolpyruvate; glycerol kinase from C. mycoderma; potassium chloride; adenosine 5'-triphosphoric acid; 2-hydroxyethanethiol; magnesium chloride; alkaline phosphatase 1.) H2O, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 4039 - 4045
反应条件
pyridine Ambient temperature;
参考文献
Curran, Dennis P.; Kim, Byeang Hyean; Piyasena, H. P.; Loncharich, R. J.; Houk, K. N.
Journal of Organic Chemistry, 1987 , vol. 52, # 11 p. 2137 - 2141
反应条件
strong acid ion exchange resin (Amberlyst 15, H+ form) in 1,4-dioxane T=100°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
SK CORPORATION
Patent: WO2007/81065 A1, 2007 ;
Location in patent: Page/Page column 6-7 ;
