反应条件
1: 0.5 g / AlCl3 / diethyl ether / 1.) 0 deg C, 3 h, 2.) 20 deg C, 3 h
2: 0.22 g / K2CO3, KI / dimethylformamide / 14 h / 65 °C
3: 0.18 g / NH4Cl, Zn moss / ethanol; H2O / 120 h / Ambient temperature
4: 1.) NaH, 2.) NaH / 1.) DMSO, room temperature, 6 days, 2.) DMSO, 50 deg C, 0.5 h
5: K2CO3 / acetone / 11 h / Heating
View Scheme
参考文献
Adams, Joyce H.; Brown, P. Margaret; Gupta, Padma; Khan, M. Shafig; Lewis, John R.
Tetrahedron, 1981 , vol. 37, p. 209 - 218
