反应条件
in acetonitrile byproducts: Zn(ReO4)2, ReO3, Zn(CH3COO)2; (inert atm.); addn. of acetic chloride to soln. of rhenium compd. in CH3CN, stirring for 10 min, filtration, addn. of zinc compd., stirring for 30 min; filtration, evapn., sublimation at 40°C at 1E-1 mbar, GC and NMR;
