反应条件
1: H2O2 / acetic acid
2: 24 percent / 65 percent HNO3, conc. H2SO4 / 3 h / 93 - 95 °C
3: 50 percent / PCl3 / CHCl3 / 8 h / Heating
4: 1) H2O2 / 1) CH3COOH, H2O, 1 h 40 deg C, 1 h 50 deg C, 1 h 70 deg C, 1 h 80 deg C, 1 h 90 deg C, 17 h 100 deg C. 2) 20 min 125 deg C, 2 h 136-140 deg C
5: 17 percent / KMnO4 / H2O / 1) 1 h, 10 deg C; 2) 30 min, 40 deg C
View Scheme
参考文献
Oehlke, J.; Schroetter, E.; Dove, S.; Schick, H.; Niedrich, H.
Pharmazie, 1983 , vol. 38, # 9 p. 591 - 596
