1-(2-异丙氧基苯基)乙酮合成路线 （共 7 条）
反应条件
1: potassium hydroxide / water; ethanol / 20 °C 2: boron trichloride / dichloromethane / 2 h / 0 °C View Scheme
参考文献
Lee, Ya-Ting; Fong, Tsorng-Harn; Chen, Hui-Min; Chang, Chao-Yuan; Wang, Yun-Hsin; Chern, Ching-Yuh; Chen, Yau-Hung
Molecules, 2014 , vol. 19, # 1 p. 641 - 650
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=70°C;
参考文献
Chen, Yau-Hung; Wang, Wei-Hua; Wang, Yun-Hsin; Lin, Zi-Yu; Wen, Chi-Chung; Chern, Ching-Yuh
Molecules, 2013 , vol. 18, # 2 p. 2052 - 2060
反应条件
potassium phosphate in dimethyl sulfoxide
T=60°C;
参考文献
Horaguchi, Takaaki; Tsukada, Chikara; Hasegawa, Eietsu; Shimizu, Takahachi; Suzuki, Tsuneo; Tanemura, Kiyoshi
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1261 - 1272
反应条件
in acetonitrile
1 h; Irradiation;
参考文献
Horaguchi, Takaaki; Tsukada, Chikara; Hasegawa, Eietsu; Shimizu, Takahachi; Suzuki, Tsuneo; Tanemura, Kiyoshi
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1261 - 1272
反应条件
1: 1) K3PO4 2) 2M aq. KOH / 1) acetone, reflux 2) EtOH
2: 54 percent / acetonitrile / 1 h / Irradiation
View Scheme
参考文献
Horaguchi, Takaaki; Tsukada, Chikara; Hasegawa, Eietsu; Shimizu, Takahachi; Suzuki, Tsuneo; Tanemura, Kiyoshi
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1261 - 1272
反应条件
1: potassium hydroxide / water; ethanol / 20 °C
2: boron trichloride / dichloromethane / 2 h / 0 °C
View Scheme
参考文献
Lee, Ya-Ting; Fong, Tsorng-Harn; Chen, Hui-Min; Chang, Chao-Yuan; Wang, Yun-Hsin; Chern, Ching-Yuh; Chen, Yau-Hung
Molecules, 2014 , vol. 19, # 1 p. 641 - 650
反应条件
1: 77 percent / sodium hydride (60percent dispersion in mineral oil) / ethanol / room temp., then reflux, 7 h
2: 67 percent / HCl / ethanol / 72 h / Ambient temperature
3: BCl3
View Scheme
参考文献
Iinuma, Munekazu; Tanaka, Toshiyuki; Hamada, Koji; Mizuno, Mizuo; Asai, Fujio; et al.
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 9 p. 3909 - 3913
