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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
70243-84-4
合成路线
（共 12 条）
1438277-47-4
→
反应条件
70243-84-4
反应条件
4-methylmorpholine N-oxide; trifluoroacetic acid in dichloromethane T=30°C; 3 h; Reagent/catalystTime;
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
1438277-47-4
→
反应条件
1438277-61-2
+
70243-84-4
反应条件
8-methylquinoline 1-oxide; methanesulfonic acid in dichloromethane T=30°C; 3 h; Reagent/catalystTimeSolvent;
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
123-75-1
四氢吡咯
+
445-27-2
2'-氟苯乙酮
→
反应条件
70243-84-4
反应条件
potassium carbonate in N,N-dimethyl-formamide T=152°C;
参考文献
Nijhuis; Verboom; Abu El-Fadl; Harkema; Reinhoudt
Journal of Organic Chemistry, 1989 , vol. 54, # 1 p. 199 - 209
110-52-1
1,4-二溴丁烷
+
551-93-9
邻氨基苯乙酮
→
反应条件
70243-84-4
反应条件
N-ethyl-N,N-diisopropylamine in toluene Heating;
参考文献
Verboom, W.; Hamzink, M. R. J.; Reinhoudt, D. N.; Visser, R.
Tetrahedron Letters, 1984 , vol. 25, # 38 p. 4309 - 4312
615-36-1
2-溴苯胺
→
反应条件
70243-84-4
反应条件
1: N-ethyl-N,N-diisopropylamine / toluene / 24 h / |Reflux 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 80 °C 3: potassium carbonate / methanol / 12 h / 20 °C 4: 4-methylmorpholine N-oxide; trifluoroacetic acid / dichloromethane / 3 h / 30 °C View Scheme
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
87698-81-5
1-(2-溴苯基)吡咯烷
→
反应条件
70243-84-4
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 80 °C 2: potassium carbonate / methanol / 12 h / 20 °C 3: 4-methylmorpholine N-oxide; trifluoroacetic acid / dichloromethane / 3 h / 30 °C View Scheme
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
615-43-0
2-碘苯胺
→
反应条件
70243-84-4
反应条件
1: N-ethyl-N,N-diisopropylamine / toluene / 24 h / |Reflux 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 20 °C 3: potassium carbonate / methanol / 12 h / 20 °C 4: 4-methylmorpholine N-oxide; trifluoroacetic acid / dichloromethane / 3 h / 30 °C View Scheme
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
1443005-29-5
→
反应条件
70243-84-4
反应条件
1: potassium carbonate / methanol / 12 h / 20 °C 2: 4-methylmorpholine N-oxide; trifluoroacetic acid / dichloromethane / 3 h / 30 °C View Scheme
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
615-36-1
2-溴苯胺
→
反应条件
1438277-61-2
+
70243-84-4
反应条件
1: N-ethyl-N,N-diisopropylamine / toluene / 24 h / |Reflux 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 80 °C 3: potassium carbonate / methanol / 12 h / 20 °C 4: methanesulfonic acid; 8-methylquinoline 1-oxide / dichloromethane / 3 h / 30 °C View Scheme
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
87698-81-5
1-(2-溴苯基)吡咯烷
→
反应条件
1438277-61-2
+
70243-84-4
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 80 °C 2: potassium carbonate / methanol / 12 h / 20 °C 3: methanesulfonic acid; 8-methylquinoline 1-oxide / dichloromethane / 3 h / 30 °C View Scheme
参考文献
Chen, Dian-Feng; Han, Zhi-Yong; He, Yu-Ping; Yu, Jie; Gong, Liu-Zhu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12307 - 12310
Angew. Chem., 2012 , vol. 124, # 49 p. 12307 - 12310,4
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