2,2,2-三氟月桂酸乙酯合成路线 （共 6 条）
反应条件
porcine pancreatic lipase; hydrogen 1.) Et2O, 78 h, 2.) 5percent Pd-C, 20.75 h; Yield given. Multistep reaction;
参考文献
Morgan, Brian; Oehlschlager, Allan C.; Stokes, Thomas M.
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3231 - 3236
反应条件
porcine pancreatic lipase in diethyl ether 72 h; Ambient temperatureenantioselectivity of transesterification; Product distributionRate constant;
参考文献
Tetrahedron Letters, , vol. 28, # 19 p. 2091 - 2094
反应条件
1: With diisobutylaluminium hydride in dichloromethane T=-78 - -60°C; 2 h; 2: With ammonia; iodine in tetrahydrofuran; dichloromethane; water T=20°C; 3 h;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
in diethyl ether 45.5 h; Ambient temperatureporcine pancreatic lipase;
参考文献
Morgan, Brian; Oehlschlager, Allan C.; Stokes, Thomas M.
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3231 - 3236
反应条件
porcine pancreatic lipase; hydrogen 1.) Et2O, 78 h, 2.) 5percent Pd-C, 20.75 h; Yield given. Multistep reaction;
参考文献
Morgan, Brian; Oehlschlager, Allan C.; Stokes, Thomas M.
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3231 - 3236
反应条件
tetrafluoroboric acid in chloroform-d1
参考文献
Koller, K. L.; Dorn, H. C.
Analytical Chemistry, 1982 , vol. 54, # 3 p. 529 - 533
