5-氧代-1,3,3-三甲基-环己烷甲腈合成路线 （共 21 条）
反应条件
titanium tetrachloride in dichloromethane
T=0°C;
参考文献
Ito, Yoshihiko; Kato, Hidehito; Imai, Hiroshi; Saegusa, Takeo
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6449 - 6450
反应条件
hydrogen cyanide in butyltrimethylammonium methylcarbonate
参考文献
BASF Aktiengesellschaft
Patent: US5516928 A1, 1996 ;
反应条件
hydrogen cyanide; nitric acid in water
参考文献
Nippon Chemicals Co., Ltd.
Patent: US5179221 A1, 1993 ;
反应条件
in toluene
T=20°C; Addition; 1.5 h;
参考文献
Dischino, Douglas D.; Cianci, Christopher; Krystal, Mark; Meanwell, Nicholas A.; Morimoto, Hiromi; Pearce, Bradley C.; Williams, Philip; Yu, Kuo-Long
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 10 p. 965 - 974
反应条件
ammonium chloride in water; N,N-dimethyl-formamide
T=80°C; 16 h;
参考文献
Pandey, Satish C.; Singh, Sudhir S.; Patro, Balaram; Ghosh, Anil C.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 12 p. 2705 - 2707
参考文献
BASF Aktiengesellschaft
Patent: US6022988 A1, 2000 ;
反应条件
in tetraethylammonium bromide
参考文献
Nippon Chemicals Co., Ltd.
Patent: US5179221 A1, 1993 ;
反应条件
methanol; acetic acid
参考文献
Whitmore; Roberts
Journal of Organic Chemistry, 1948 , vol. 13, p. 31,34
反应条件
ammonia in methanol
Internal standard: triethylene glycol dimethyl ether (triglyme);
参考文献
RHODIA CHIMIE
Patent: WO2004/60866 A2, 2004 ;
Location in patent: Page 13 ;
反应条件
hydrogenchloride; water
Reflux;
参考文献
Chen, Li; Lin, Xianfeng; Qiu, Zongxing; Tang, Guozhi; Wang, Lisha; Wu, Jim Zhen; Yang, Wengang
Patent: US2011/195979 A1, 2011 ;
Location in patent: Page/Page column 40 ;
