boron trichloride; chlorobenzene
durch Sublimation des Reaktionsprodukts im Hochvakuum bei 60grad;
参考文献
Ryschkewitsch et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 4515
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Hohnstedt; Haworth
Journal of the American Chemical Society, 1960 , vol. 82, p. 89,92
in neat (no solvent)
byproducts: (C6H5)(CH3)2SiCl; dry N2 atmosphere; heating (sealed tube, 95°C);
参考文献
Bowser, James R.; Marohn, Kristina F.; Gilbert, Stephanie R.; Robbins, Andrea M.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 9 p. 1559 - 1566
in melt
byproducts: (NPCl2)n; heating in melt; (11)B-NMR and mass spectroscopy, thermogravimetric anal.;
参考文献
Ziembinski, Ralf; Honeyman, Charles; Mourad, Ophyr; Foucher, Dan; Rulkens, Rudy; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 76, # 1-4 p. 219 - 222
