N-(2-甲氧基苯基)-3-吡啶甲酰胺合成路线 （共 6 条）
反应条件
anhydrous iron chloride; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=135°C; 24 h; Inert atmosphere;
参考文献
Correa, Arkaitz; Elmore, Simon; Bolm, Carsten
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3527 - 3529
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl
T=150°C; 72 h; Inert atmosphere;
参考文献
Romero; Harrak; Basset; Orue; Pujol
Tetrahedron, 2009 , vol. 65, # 10 p. 1951 - 1956
反应条件
1: SOCL2 / 2 h / Heating
2: triethylamine / benzene / 10 h / Heating
View Scheme
参考文献
Bukhtiarova; Trinus; Danilenko; Ovrutskii; Sharykina
Pharmaceutical Chemistry Journal, 1998 , vol. 32, # 11 p. 597 - 599
反应条件
acetic acid
T=100°C; 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Harrington, Philip M.
Heterocycles, 1993 , vol. 35, # 2 p. 683 - 687
反应条件
triethylamine in benzene
Acylation; 10 h; Heating;
参考文献
Bukhtiarova; Trinus; Danilenko; Ovrutskii; Sharykina
Pharmaceutical Chemistry Journal, 1998 , vol. 32, # 11 p. 597 - 599
参考文献
Calo; Evdokimoff
Gazzetta Chimica Italiana, 1950 , vol. 80, p. 456,460
